Vanoxerine-dihydrochloride-LCMS-11420-MedChemExpress

MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\CPK\\CPK2016-N16-11420.D Tgt Mass (EZX): 450.50 Injection Date : 17 Nov 16 4:18 pm +0800 Seq. Line : 0 Sample Name : CPK2016-N16-11420 Location : P2-D-02 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No: HY-13217 Batch#11420 Easy-Access Method: '1-POS-3MIN' 450.50 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C *DAD1 B, Sig=214,4 Ref=off mAU8006004001.32520000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 703000002500002000001500001000005000000.511.5 Ion 451.5, MSD1 451.5,Target Mass 450.5 +H Positive, EIC=451.2:452.2 17500015000012500010000075000500002500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.47622.5min1.4791.51.47622.5min*1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.32 0.02 3.42 2.96 0.36 130 1.48 0.02 945.53 937.93 99.64 451HY-LCMS-02 11/17/2016 16:29:08 KFF(LCMS-02)Page 1 of 2

MS Report from Instrument: HY-LCMS-02

Ret. Time: 1.48 <<<< POSITIVE SPECTRA >>>> ES-API Positive45000400003500030000200001000050000200300400500600700800900m/z 203.1 249.315000 452.425000 451.4HY-LCMS-02 11/17/2016 16:29:08 KFF(LCMS-02)Page 2 of 2