ETP-46464_LCMS_10307_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.DSample Name: CPK2015-924-10307=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 20Acq. Instrument : HY-LCMS-02 Location : P1-B-07Injection Date : 9/24/2015 10:42:17 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 9/24/2015 9:08:31 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HY-340_9-H01RS06(RP-HPLC).MLast changed : 9/24/2015 2:08:11 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : MS:100-1000,Column ID:A-RP-108,30℃ Catalog No : HY-15521 Batch#10307 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 B, Sig=214,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.D) 2.469 1.760 1.957 2.095 2.177 2.307mAU20001500100050000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.760 MM 0.0574 11.14335 3.23503 0.1567 2 1.957 MM 0.0438 6.38909 2.43042 0.0898 3 2.095 MM 0.0601 5.72667 1.58861 0.0805 4 2.177 MM 0.0394 1.82320 7.70786e-1 0.0256 5 2.307 MM 0.0559 21.53548 6.41974 0.3028 6 2.469 MM 0.0513 7066.62012 2295.83008 99.3446 Totals : 7113.23792 2310.27467 ===================================================================== *** End of Report ***HY-LCMS-02 9/24/2015 2:08:13 PM Yang Qian(LCMS-02)Page 1 of 1

Data File D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.DSample Name: CPK2015-924-10307=====================================================================Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 20Acq. Instrument : HY-LCMS-02 Location : P1-B-07Injection Date : 9/24/2015 10:42:17 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 9/24/2015 9:08:31 AM by Yang Qian(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\HY-340_9-H01RS06(RP-HPLC).MLast changed : 9/24/2015 2:09:20 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : MS:100-1000,Column ID:A-RP-108,30℃ Catalog No : HY-15521 Batch#10307 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.D) ES-API, Pos, Sc 2.47860000050000040000030000020000010000000.511.522.53min HY-LCMS-02 9/24/2015 2:09:22 PM Yang Qian(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.DSample Name: CPK2015-924-10307MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 2.478 3293700 472.10 I 471.15 I 236.15 I*MSD1 SPC, time=2.455:2.509 of D:\\AGLIENT 1260\\DATA\\20150924\\20150924 2015-09-24 09-08-31\\CPK2015-924-10307.D ES-API100806040200100200300400500600700800900m/z 471.1Max: 277984 236.1 *** End of Report ***HY-LCMS-02 9/24/2015 2:09:22 PM Yang Qian(LCMS-02) 473.1 472.1Page 2 of 2